The Influence of Biological Fluids on Crack Spacing Distribution in Si-DLC Films on Steel Substrates

AA Ogwu, T Coyle, TIT Okpalugo, P Kearney, PD Maguire, JAD McLaughlin

Research output: Contribution to journalArticle

32 Citations (Scopus)

Abstract

An experimental investigation of the effect of exposure to biological fluids on the adhesion of silicon modified DLC films to steel substrates (304 stainless and mild steel) was conducted. The substrate straining test was used for the adhesion measurement. A statistical procedure, which is faster and more reliable than the ab initio computer simulation of crack spacing distribution adopted by previous authors in the literature was used to treat the crack spacing data. We observed a change in the crack spacing distribution from the Weibull for the as-prepared films to Lognormal for the films immersed in biological fluids. A reduction in the interfacial adhesion values was also observed for the films soaked in biological fluids compared to the as-prepared films. The proposed approach can be used when the crack spacing matches other statistical distributions. (C) 2003 Acta Materialia Inc. Published by Elsevier Science Ltd. All rights reserved.
LanguageEnglish
Pages3455-3465
JournalActa Materialia
Volume51
Issue number12
DOIs
Publication statusPublished - Jul 2003

Fingerprint

Steel
Cracks
Fluids
Substrates
Adhesion
Silicon
Carbon steel
Stainless steel
Computer simulation

Keywords

  • thin films
  • coating
  • tension test

Cite this

Ogwu, AA ; Coyle, T ; Okpalugo, TIT ; Kearney, P ; Maguire, PD ; McLaughlin, JAD. / The Influence of Biological Fluids on Crack Spacing Distribution in Si-DLC Films on Steel Substrates. In: Acta Materialia. 2003 ; Vol. 51, No. 12. pp. 3455-3465.
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The Influence of Biological Fluids on Crack Spacing Distribution in Si-DLC Films on Steel Substrates. / Ogwu, AA; Coyle, T; Okpalugo, TIT; Kearney, P; Maguire, PD; McLaughlin, JAD.

In: Acta Materialia, Vol. 51, No. 12, 07.2003, p. 3455-3465.

Research output: Contribution to journalArticle

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AB - An experimental investigation of the effect of exposure to biological fluids on the adhesion of silicon modified DLC films to steel substrates (304 stainless and mild steel) was conducted. The substrate straining test was used for the adhesion measurement. A statistical procedure, which is faster and more reliable than the ab initio computer simulation of crack spacing distribution adopted by previous authors in the literature was used to treat the crack spacing data. We observed a change in the crack spacing distribution from the Weibull for the as-prepared films to Lognormal for the films immersed in biological fluids. A reduction in the interfacial adhesion values was also observed for the films soaked in biological fluids compared to the as-prepared films. The proposed approach can be used when the crack spacing matches other statistical distributions. (C) 2003 Acta Materialia Inc. Published by Elsevier Science Ltd. All rights reserved.

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