Abstract
Language | English |
---|---|
Pages | 365-373 |
Journal | POLYMERS & POLYMER COMPOSITES |
Volume | 16 |
Issue number | 6 |
Publication status | Published - 2008 |
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Keywords
- Thermoplastic resin
- Process monitoring
- Dielectric analysis.
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Monitoring the Degree of Conversion of Cyclic Butylene Terephthalate using Dielectric Analysis. / Archer, E; McIlhagger, AT; McIlhagger, R; Quinn, JP; Mallon, P; Bradaigh, CO.
In: POLYMERS & POLYMER COMPOSITES, Vol. 16, No. 6, 2008, p. 365-373.Research output: Contribution to journal › Article
TY - JOUR
T1 - Monitoring the Degree of Conversion of Cyclic Butylene Terephthalate using Dielectric Analysis
AU - Archer, E
AU - McIlhagger, AT
AU - McIlhagger, R
AU - Quinn, JP
AU - Mallon, P
AU - Bradaigh, CO
PY - 2008
Y1 - 2008
N2 - Dielectric analysis (DEA) is the most common technique used to determine the state of cure in-process for many thermosetting resins systems such as epoxies, polyesters, polyurethanes, polyimides, silicones, bismaleimides, and phenolics. The objective of this work is to investigate the processing characteristics of cyclic butylene terephthalate (CBT) (supplied by Cyclics Corporation) which polymerises to form a thermoplastic, polybutylene terephthalate (PBT). This paper reports on the interim results of ongoing experimental investigations in which DEA is used to correlate the process cycle to composite structural features and mechanical performance of a complex composite part. Through adjustments in process cycle, the significant processing parameters have been identified which optimise the production of thermoplastic PBT composite parts. The recorded ion viscosity is used to indicate change in material viscosity, conversion rate and process time. These results have been analysed and presented as a guide for correct process control.
AB - Dielectric analysis (DEA) is the most common technique used to determine the state of cure in-process for many thermosetting resins systems such as epoxies, polyesters, polyurethanes, polyimides, silicones, bismaleimides, and phenolics. The objective of this work is to investigate the processing characteristics of cyclic butylene terephthalate (CBT) (supplied by Cyclics Corporation) which polymerises to form a thermoplastic, polybutylene terephthalate (PBT). This paper reports on the interim results of ongoing experimental investigations in which DEA is used to correlate the process cycle to composite structural features and mechanical performance of a complex composite part. Through adjustments in process cycle, the significant processing parameters have been identified which optimise the production of thermoplastic PBT composite parts. The recorded ion viscosity is used to indicate change in material viscosity, conversion rate and process time. These results have been analysed and presented as a guide for correct process control.
KW - Thermoplastic resin
KW - Process monitoring
KW - Dielectric analysis.
M3 - Article
VL - 16
SP - 365
EP - 373
JO - Polymers and Polymer Composites
T2 - Polymers and Polymer Composites
JF - Polymers and Polymer Composites
SN - 0967-3911
IS - 6
ER -