Application of electrospray mass spectrometry in the detection and determination of Remazol textile dyes

Franklin Smyth, Stephen McClean, EJ O'Kane, Ibrahim Banat, Geoffrey McMullan

Research output: Contribution to journalArticle

26 Citations (Scopus)

Abstract

The electrospray (ES) behaviour of selected Remazol textile dyes, their hydrolysis products and the latters' reaction, following elution from a strong anion-exchange cartridge, with 30% concentrated HCl in MeOH, is studied and applied to the direct analysis of dye containing effluent. For unambiguous identification and determination of these textile dyes in effluents, it is necessary to resort to ES utilising MS-MS and MS3. Further, a tabular review of recent applications of HPLC-ES-MS and, to a lesser extent, CE-ES-MS with reference to drug and pesticide analysis is presented. (C) 1999 Elsevier Science B.V. AII rights reserved.
LanguageEnglish
Pages259-274
JournalJOURNAL OF CHROMATOGRAPHY A
Volume854
Issue number1-2
Publication statusPublished - Aug 1999

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Mass spectrometry
Textiles
Coloring Agents
Effluents
Pesticides
Anions
Hydrolysis
Pharmaceutical Preparations

Cite this

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title = "Application of electrospray mass spectrometry in the detection and determination of Remazol textile dyes",
abstract = "The electrospray (ES) behaviour of selected Remazol textile dyes, their hydrolysis products and the latters' reaction, following elution from a strong anion-exchange cartridge, with 30{\%} concentrated HCl in MeOH, is studied and applied to the direct analysis of dye containing effluent. For unambiguous identification and determination of these textile dyes in effluents, it is necessary to resort to ES utilising MS-MS and MS3. Further, a tabular review of recent applications of HPLC-ES-MS and, to a lesser extent, CE-ES-MS with reference to drug and pesticide analysis is presented. (C) 1999 Elsevier Science B.V. AII rights reserved.",
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Application of electrospray mass spectrometry in the detection and determination of Remazol textile dyes. / Smyth, Franklin; McClean, Stephen; O'Kane, EJ; Banat, Ibrahim; McMullan, Geoffrey.

In: JOURNAL OF CHROMATOGRAPHY A, Vol. 854, No. 1-2, 08.1999, p. 259-274.

Research output: Contribution to journalArticle

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T1 - Application of electrospray mass spectrometry in the detection and determination of Remazol textile dyes

AU - Smyth, Franklin

AU - McClean, Stephen

AU - O'Kane, EJ

AU - Banat, Ibrahim

AU - McMullan, Geoffrey

N1 - 15th Montreux Symposium on LC-MS, SFC-MS, CE-MS and MS-MS, MONTREUX, FRANCE, NOV 11-13, 1998

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AB - The electrospray (ES) behaviour of selected Remazol textile dyes, their hydrolysis products and the latters' reaction, following elution from a strong anion-exchange cartridge, with 30% concentrated HCl in MeOH, is studied and applied to the direct analysis of dye containing effluent. For unambiguous identification and determination of these textile dyes in effluents, it is necessary to resort to ES utilising MS-MS and MS3. Further, a tabular review of recent applications of HPLC-ES-MS and, to a lesser extent, CE-ES-MS with reference to drug and pesticide analysis is presented. (C) 1999 Elsevier Science B.V. AII rights reserved.

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